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Project

Study by monocrystal X-ray diffraction :obtention of the tridimensional structure and characterisation

Duration

1990-2006

Keywords

X-ray diffraction tridimensional structure

Description

This service includes: the crystallisation of compounds, in order to obtain monocrystals the resolution of the X-ray diffraction spectrum, to obtain the tridimensional structure and its analysis.

Research unit(s)

Staff (finished contracts)

Chairperson(s)
François DURANT Leader
Johan WOUTERS Leader 081/724550

Research staff
Fabrice CAMUS Researcher
Bernadette NORBERG Researcher 081/725457

Publications (21)

Papers

2003
Versatile access to benzhydryl-phenylureas through an unexpected rearrangement during microwave-enhanced synthesis of hydantoins, in Organic letters, volume 5, issue 20, pp. 3599-3602
Giulio MUCCIOLI, Johan WOUTERS, Jacques POUPAERT, Bernadette NORBERG, Wolfgang POPPITZ, Gerhard SCRIBA, Didier LAMBERT
2003
8,8'-Dichloro-1,1',5,5'-tetrahydro-10,10'-bipyrrolo[1,2-b]isoquinoline-3,3'(2H,2'H)-dione, in Acta crystallographica. Section E: Structure reports, volume E59, pp. 1002-1003
Fabrice CAMUS, Bernadette NORBERG, Anne BOURRY, Rufine AKUÉ-GÉDU, Benoît RIGO, François DURANT
2003
A rapid and efficient microwave-assisted synthesis of hydantoins and thiohydantoins, in Tetrahedron, volume 59, pp. 1301-1307
Giulio MUCCIOLI, Jacques POUPAERT, Johan WOUTERS, Bernadette NORBERG, Wolfgang POPPITZ, Gerhard SCRIBA, Didier LAMBERT
2002
4-Methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazino]thiazole and its reduction product, 4-methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazono]-4,5-dihydrothiazole, in Acta crystallographica. Section C: Crystal structure communications, volume C, issue 58, pp. 69-71
Johan WOUTERS, Bernadette NORBERG, Salvatore GUCCIONE
2002
Microwave promoted synthesis of 4,7-dihydro-1H-imidazo[4,5-e]-1,2,4-triazepin-8-ones as ring-expanded hypoxanthine analogues, in Synlett, issue 3, pp. 519-521
Pierre RABOISSON, Bernadette NORBERG, J. Richard CASIMIR, Jean-Jacques BOURGUIGNON
2002
Studies on Pyrrolidinones : Some Attempts to Improve the Synthesis of Methyl N-(3,4,4',5-Tetramethoxybenzhydryl)pyroglutamate (HEI81) by Using N-Acyl Iminium Salts Methodologies., in Journal of Heterocyclic Chemistry, volume 39, pp. 109-118
Anne BOURRY, Franck PITARD, Benoît RIGO, Gérard SANZ, Fabrice CAMUS, Bernadette NORBERG, François DURANT, Daniel COUTURIER
2001
1,1'-(4-Methylbenzylidene)bis(5-oxopyrrolidine-2-carboxylic acid), in Acta Crystallographica , volume 57, pp. o439-o440
Fabrice CAMUS, Bernadette NORBERG, Anne BOURRY, Benoît RIGO, François DURANT
2000
Molecular analysis of the Beta-polymorphic form of trielaidin: crystal structure at low temperature, in Acta crystallographica. Section B, issue B56, pp. 317-321
Christine CULOT, Bernadette NORBERG, Guy EVRARD, François DURANT
2000
Structural analysis of pyrrolidinones, in Acta crystallographica. Section C. Crystal structure communications, volume C, issue 56, pp. 193-196
Bernadette NORBERG, Fabrice CAMUS, Anne LEGRAND, Benoît RIGO, François DURANT, Johan WOUTERS
2000
7-Nitroindazole, in Acta crystallographica. Section C: Crystal structure communications, issue 56
Frédéric OOMS, Bernadette NORBERG, Emre ISIN, Neal CASTAGNOLI, Cornelis VAN DER SCHYF, Johan WOUTERS
2000
Terbogrel, a dual-acting agent for thromboxane receptor antagonism and thromboxane synthase inhibition, in Acta crystallographica Section C: Crystal Structure communications, issue 56, pp. 1265-1266
Catherine MICHAUX, Bernadette NORBERG, Jean-Michel DOGNÉ, François DURANT, Bernard MASEREEL, Jacques DELARGE, Johan WOUTERS
2000
Structural Analysis of Pyrrolidinones, in Acta Crystallographica , volume 56, pp. 193-196
Fabrice CAMUS, Bernadette NORBERG, Anne LEGRAND, Benoît RIGO, François DURANT, Johan WOUTERS
2000
Studies on pyrrolidinones: synthesis and cyclization of N-[α-naphthyl-(3,4,5-trimethoxyphenyl)-methyl]pyroglutamic acid, in Journal of heterocyclic chemistry, volume 37, issue 37, pp. 215
Anne LEGRAND, Benoît RIGO, Jean-Pierre HÉNICHART, Bernadette NORBERG, Fabrice CAMUS, François DURANT, Daniel COUTURIER
1998
A dinitrobenzoate derivative of an a-methoxy-y-hydroxysilane, in Acta crystallographica. Section C: Crystal structure communications, issue C54, pp. 1944-1945
Guy BAUDOUX, Bernadette NORBERG, Jamal BOUSBAA, Alain KRIEF, Guy EVRARD
1998
Three intermediates in the synthesis of Chrysantemic acid, in Acta crystallographica. Section C, issue 54, pp. 834-837
Guy BAUDOUX, Bernadette NORBERG, Laurent PROVINS, Alexandre FROIDBISE, Alain KRIEF, Guy EVRARD
1998
Dinitrobenzoate derivative of a chiral arylcyclopentane, in Acta crystallographica C, issue 54, pp. 1353-1355
Guy BAUDOUX, Bernadette NORBERG, Jamal BOUSBAA, Alain KRIEF, Guy EVRARD
1998
Synthesis and absolute structure determination of Camphanoate derivatives of five Bicyclo[3.1.0]hexane compounds, in Acta crystallographica. Section C, issue 54, pp. 392-398
Alain KRIEF, Thierry OLLEVIER, Dominique SWINNEN, Bernadette NORBERG, Guy BAUDOUX, Guy EVRARD
1998
Cis-4,6-Dimethyl-2-phenyl-1,3-diselenane, in Acta crystallographica. Section C, issue 54, pp. 1505-1507
Guy BAUDOUX, Bernadette NORBERG, Johan WOUTERS, Laurent DEFRERE, Alain KRIEF, Guy EVRARD
1997
Synthesis of 3-Phenylindoline-2-carboxamides as semi-rigid phenylalanine mimetics, in Tetrahedron letters, volume 38, issue 46, pp. 8033-8036
Valérie COLLOT, Martine SCHMITT, Ashok K. MARWAH, Bernadette NORBERG, Jean-Jacques BOURGUIGNON
1997
Trans- and cis-S-C-C-S conformations in 5-(2,2'-Dithien-5-yl)-2'-deoxyuridine, in Acta crystallographica. Section C, issue 53, pp. 892-895
Johan WOUTERS, I. CREUVEN, Bernadette NORBERG, Guy EVRARD, François DURANT, A. VAN AERSCHOT, P. HERDEWIJN
1997
The dipeptide pGlu-Pro-NH2, in Acta crystallographica. Section C, issue 53, pp. 477-480
Johan WOUTERS, Bernadette NORBERG, Guy EVRARD

Collaborations

  • FUNDP, Chimie organique de synthèse
  • Hautes Etudes Industrielles, Laboratoire de Synthèses Organiques
  • UCB (Chemin du Foriest), Developpement Pharmaceutique

Contracts

  • UCB (Chemin du Foriest), Developpement Pharmaceutique